C₃₃H₂₇BF₂N₂O₄

Base Information

Chemical Name:C₃₃H₂₇BF₂N₂O₄
CAS No.:168021-22-5
Molecular Formula:C₃₃H₂₇BF₂N₂O₄
Molecular Weight:564.396
Hs Code.:

C<sub>33</sub>H<sub>27</sub>BF<sub>2</sub>N<sub>2</sub>O<sub>4</sub>

Synonyms:C₃₃H₂₇BF₂N₂O₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₃₃H₂₇BF₂N₂O₄

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Technology Process of C₃₃H₂₇BF₂N₂O₄

There total 5 articles about C₃₃H₂₇BF₂N₂O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 168021-21-4
C₃₃H₂₈N₂O₄

: 168021-22-5
C₃₃H₂₇BF₂N₂O₄

Guidance literature:: With boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; Inert atmosphere;
DOI:10.1021/jo200246q

Reference yield:

: 168021-39-4
C₁₇H₁₆O₄

: 168021-22-5
C₃₃H₂₇BF₂N₂O₄

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium hydroxide / methanol; water; acetic acid / 24 h / 20 °C

2: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

With ammonium hydroxide; boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jo200246q

Reference yield:

: C₁₇H₁₈N₂O₄

: 168021-22-5
C₃₃H₂₇BF₂N₂O₄

Guidance literature:: Multi-step reaction with 3 steps

1: lead(IV) tetraacetate / tetrahydrofuran / 1 h / 25 °C / Inert atmosphere

2: ammonium hydroxide / methanol; water; acetic acid / 24 h / 20 °C

3: boron trifluoride diethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere

With ammonium hydroxide; boron trifluoride diethyl etherate; lead(IV) tetraacetate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; acetic acid;
DOI:10.1021/jo200246q