Technology Process of C51H79NO16S
There total 3 articles about C51H79NO16S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
C52H81NO16S;
With
sodium acetate;
In
methanol; water;
at 20 ℃;
for 0.166667h;
With
iodine;
In
methanol; water;
at 25 - 30 ℃;
for 2h;
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide / acetone / 2.5 h / 20 °C / Inert atmosphere
2.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 5 °C / Inert atmosphere; Ice cooling
3.1: sodium acetate / methanol; water / 0.17 h / 20 °C
3.2: 2 h / 25 - 30 °C
With
sodium acetate; sodium hydride; 1,8-diazabicyclo[5.4.0]undec-7-ene; sodium iodide;
In
methanol; water; N,N-dimethyl-formamide; acetone; mineral oil;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium hydride / N,N-dimethyl-formamide; mineral oil / 3 h / 0 - 5 °C / Inert atmosphere; Ice cooling
2.1: sodium acetate / methanol; water / 0.17 h / 20 °C
2.2: 2 h / 25 - 30 °C
With
sodium acetate; sodium hydride;
In
methanol; water; N,N-dimethyl-formamide; mineral oil;