1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

Base Information

Chemical Name:1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose
CAS No.:1451958-64-7
Molecular Formula:C₃₀H₃₂O₅
Molecular Weight:472.581
Hs Code.:

Synonyms:1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

Chemical Property:

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Technology Process of 1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

There total 3 articles about 1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: lithium acetylide ethylenediamine complex

: 1451958-67-0
C₃₅H₃₈O₈S

: 1451958-64-7
1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

Guidance literature:: In tetrahydrofuran; at 20 ℃; for 9h; Inert atmosphere;
DOI:10.1016/j.bmc.2013.05.034

Reference yield:

: (2R,3S,5S)-2-[Bis-(4-methoxy-phenyl)-phenyl-methoxymethyl]-5-(2-hydroxy-ethyl)-tetrahydro-furan-3-ol

: 1451958-64-7
1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 2 steps

1: pyridine / 12 h / 20 °C / Inert atmosphere

2: tetrahydrofuran / 9 h / 20 °C / Inert atmosphere

With pyridine; In tetrahydrofuran;
DOI:10.1016/j.bmc.2013.05.034

Reference yield:

: 197784-38-6
ethyl [2-deoxy-5-O-(4,4'-dimethoxytrityl)-β-D-erythro-pentofuranosyl]acetate

: 1451958-64-7
1-(1-butyn-4-yl)-1,2-dideoxy-5-O-(4,4'-dimethoxytrityl)-β-D-ribofuranose

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium tetrahydride / tetrahydrofuran / Inert atmosphere

2: pyridine / 12 h / 20 °C / Inert atmosphere

3: tetrahydrofuran / 9 h / 20 °C / Inert atmosphere

With pyridine; lithium aluminium tetrahydride; In tetrahydrofuran;
DOI:10.1016/j.bmc.2013.05.034