2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

Base Information

Chemical Name:2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester
CAS No.:848693-94-7
Molecular Formula:C₃₄H₃₄N₆O₆S
Molecular Weight:654.747
Hs Code.:

2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1<i>H</i>-1,3a,10-triaza-benzo[<i>f</i>]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[<i>f</i>]azulene-1-carboxylic acid methyl ester

Synonyms:2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

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Chemical Property of 2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

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Technology Process of 2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

There total 6 articles about 2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2,7-diamino-oct-4-ynedioic acid diethyl ester; compound with GENERIC INORGANIC NEUTRAL COMPONENT

: 848693-94-7
2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: H₂ / Pd/C / methanol / 0.75 h / 20 °C

2: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 3 h / 0 - 20 °C

3: phosphate buffer / CH₂Cl₂; H₂O / 5 h / pH 9

4: NaOH / methanol; H₂O / 22 h

5: ethyldiisopropylamine; TBTU / CH₂Cl₂ / 20 °C

With sodium hydroxide; phosphate buffer; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; dichloromethane; water;
DOI:10.1002/anie.200462069

Reference yield:

: 848693-97-0
2,7-bis-(benzhydrylidene-amino)-oct-4-ynedioic acid diethyl ester

: 848693-94-7
2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

Guidance literature:: Multi-step reaction with 6 steps

1: HCl / diethyl ether; H₂O / 14 h / 20 °C

2: H₂ / Pd/C / methanol / 0.75 h / 20 °C

3: 1,8-diazabicyclo[5.4.0]undec-7-ene / CH₂Cl₂ / 3 h / 0 - 20 °C

4: phosphate buffer / CH₂Cl₂; H₂O / 5 h / pH 9

5: NaOH / methanol; H₂O / 22 h

6: ethyldiisopropylamine; TBTU / CH₂Cl₂ / 20 °C

With hydrogenchloride; sodium hydroxide; phosphate buffer; hydrogen; O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; 1,8-diazabicyclo[5.4.0]undec-7-ene; N-ethyl-N,N-diisopropylamine; palladium on activated charcoal; In methanol; diethyl ether; dichloromethane; water;
DOI:10.1002/anie.200462069

Reference yield:

: 848694-02-0
2-benzenesulfonylamino-7-methoxycarbonylamino-octanedioic acid

: 2,5-dihydro-3-(methylthio)-1H-2,4-benzodiazepine

: 848693-94-7
2-[4-(1-benzenesulfonyl-3-oxo-2,3,4,9-tetrahydro-1H-1,3a,10-triaza-benzo[f]azulen-2-yl)-butyl]-3-oxo-2,3,4,9-tetrahydro-1,3a,10-triaza-benzo[f]azulene-1-carboxylic acid methyl ester

Guidance literature:: With O-(benzotriazol-1-yl)-N,N,N',N'-tetramethyluronium tetrafluoroborate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃;
DOI:10.1002/anie.200462069