4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

Base Information

Chemical Name:4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde
CAS No.:1257999-67-9
Molecular Formula:C₂₁H₁₄BrF₃O₅S
Molecular Weight:515.304
Hs Code.:

Synonyms:4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

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Chemical Property of 4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

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Technology Process of 4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

There total 4 articles about 4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

: 1257999-38-4
4-hydroxy-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

: 98-58-8
4-bromobenzenesulfonyl chloride

: 1257999-67-9
4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

Guidance literature:: With N-ethyl-N,N-diisopropylamine; In N,N-dimethyl-formamide; at 0 - 20 ℃; for 3h;
DOI:10.1016/j.bmcl.2010.08.130

Reference yield:

: 1257999-32-8
4-methoxymethoxy-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

: 1257999-67-9
4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; water / tetrahydrofuran / 2 h / 50 °C

2: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With hydrogenchloride; water; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.5012/bkcs.2011.32.1.31

Reference yield:

: 95-01-2
2,4-Dihydroxybenzaldehyde

: 1257999-67-9
4-(4-bromobenzenesulfonyloxy)-2-[4-(trifluoromethyl)benzyloxy]benzaldehyde

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / acetone / 4 h / 0 - 20 °C

2: potassium carbonate / N,N-dimethyl-formamide / 20 °C

3: hydrogenchloride; water / tetrahydrofuran / 2 h / 50 °C

4: N-ethyl-N,N-diisopropylamine / N,N-dimethyl-formamide / 2 h / 0 - 20 °C

With hydrogenchloride; water; potassium carbonate; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; N,N-dimethyl-formamide; acetone;
DOI:10.5012/bkcs.2011.32.1.31