3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

Base Information

Chemical Name:3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone
CAS No.:215957-74-7
Molecular Formula:C₂₇H₃₀N₂O₂S
Molecular Weight:446.613
Hs Code.:

Synonyms:3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

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Chemical Property of 3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

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Technology Process of 3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

There total 5 articles about 3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1576-35-8
toluene-4-sulfonic acid hydrazide

: 215957-68-9
3,3-Di(2-phenylethyl)cyclobutanone

: 215957-74-7
3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: In tetrahydrofuran;

Reference yield:

: 35225-79-7
dibenzylideneacetone

: 215957-74-7
3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: Multi-step reaction with 5 steps

1: 69 percent / Hydrogen; AcOH / Platinum dioxide / ethyl acetate / 1 h / 2625.21 Torr

2: 68 percent / Sodium hydride / dimethylsulfoxide / 2 h / 50 °C

3: 37 percent / zinc dust / diethyl ether / 1 h / sonication

4: 86 percent / zinc dust / acetic acid / 0.83 h / 70 °C

5: 75 percent / tetrahydrofuran

With hydrogen; sodium hydride; acetic acid; zinc; platinum(IV) oxide; In tetrahydrofuran; diethyl ether; acetic acid; dimethyl sulfoxide; ethyl acetate; 1: Hydrogenation / 2: Wittig reaction / 3: Cycloaddition / 4: Dehalogenation / 5: Condensation;

Reference yield:

: 17486-87-2
(3-methylenepentane-1,5-diyl)dibenzene

: 215957-74-7
3,3-Di(2-phenylethyl)cyclobutanone toluene-p-sulfonylhydrazone

Guidance literature:: Multi-step reaction with 3 steps

1: 37 percent / zinc dust / diethyl ether / 1 h / sonication

2: 86 percent / zinc dust / acetic acid / 0.83 h / 70 °C

3: 75 percent / tetrahydrofuran

With zinc; In tetrahydrofuran; diethyl ether; acetic acid; 1: Cycloaddition / 2: Dehalogenation / 3: Condensation;