(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

Base Information

Chemical Name:(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol
CAS No.:595559-83-4
Molecular Formula:C₁₇H₂₅NO₄
Molecular Weight:307.39
Hs Code.:

Synonyms:(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

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Chemical Property of (2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

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Technology Process of (2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

There total 3 articles about (2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

: 444911-54-0
(3aR,4R,6aR)-N-benzyl-tetrahydro-N-hydroxy-2,2-dimethylfuro[3,4-d]-1,3-dioxol-4-amine

: 1730-25-2
allylmagnesium bromide

: 595559-83-4
(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

: (2R,3S,4R)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

Guidance literature:: In tetrahydrofuran; diethyl ether; at -30 ℃; for 3.5h;
DOI:10.1016/S0040-4020(03)00631-8

Reference yield:

: 189996-60-9
2,3-O-isopropylidene-D-erythrose

: 595559-83-4
(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 0.75 h / 110 °C

2: 88 percent / diethyl ether; tetrahydrofuran / 3.5 h / -30 °C

In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(03)00631-8

Reference yield:

: 622-30-0
N-benzyl hydroxylalmine

: 595559-83-4
(2R,3S,4S)-4-N-benzylhydroxylamino-2,3-O-isopropylidene-5-vinyl-1,2,3-pentanetriol

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / 0.75 h / 110 °C

2: 88 percent / diethyl ether; tetrahydrofuran / 3.5 h / -30 °C

In tetrahydrofuran; diethyl ether;
DOI:10.1016/S0040-4020(03)00631-8