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3β-benzoyltropane

Base Information
  • Chemical Name:3β-benzoyltropane
  • CAS No.:77850-55-6
  • Molecular Formula:C15H19NO
  • Molecular Weight:229.322
  • Hs Code.:
3β-benzoyltropane

Synonyms:3β-benzoyltropane

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Chemical Property of 3β-benzoyltropane
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Technology Process of 3β-benzoyltropane

There total 8 articles about 3β-benzoyltropane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
sodium methoxide-d3; In d(4)-methanol; at 25 ℃; for 1.5h;
Guidance literature:
Multi-step reaction with 6 steps
1: 44 percent / polyphosphoric acid / 150 °C
2: 92 percent / H2O / 3 h / Heating
3: thionyl chloride / 1 h / Heating
4: 60 percent / AlCl3 / 3.5 h / Heating
5: 0.8 g / H2 / PtO2 / ethanol / 5 h / 760 Torr
6: 100 percent / sodium methoxide-d3 / tetradeuteriomethanol / 1.5 h / 25 °C
With aluminium trichloride; thionyl chloride; PPA; hydrogen; platinum(IV) oxide; sodium methoxide-d3; In ethanol; d(4)-methanol; water;
Guidance literature:
Multi-step reaction with 5 steps
1: 92 percent / H2O / 3 h / Heating
2: thionyl chloride / 1 h / Heating
3: 60 percent / AlCl3 / 3.5 h / Heating
4: 0.8 g / H2 / PtO2 / ethanol / 5 h / 760 Torr
5: 100 percent / sodium methoxide-d3 / tetradeuteriomethanol / 1.5 h / 25 °C
With aluminium trichloride; thionyl chloride; hydrogen; platinum(IV) oxide; sodium methoxide-d3; In ethanol; d(4)-methanol; water;
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