(2S)-2--3-phenylpropyl (E)-3-pentenoate

Base Information

Chemical Name:(2S)-2--3-phenylpropyl (E)-3-pentenoate
CAS No.:221134-15-2
Molecular Formula:C₂₀H₂₇NO₃
Molecular Weight:329.439
Hs Code.:

(2S)-2-<methyl((E)-3-pentenoyl)amino>-3-phenylpropyl (E)-3-pentenoate

Synonyms:(2S)-2--3-phenylpropyl (E)-3-pentenoate

Suppliers and Price of (2S)-2--3-phenylpropyl (E)-3-pentenoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of (2S)-2--3-phenylpropyl (E)-3-pentenoate

Chemical Property:

Purity/Quality:: 98% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of (2S)-2--3-phenylpropyl (E)-3-pentenoate

There total 1 articles about (2S)-2--3-phenylpropyl (E)-3-pentenoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 90.0%

: 17066-20-5,123700-03-8
3-pentenoyl chloride

: 84773-29-5
(S)-(+)-2-(N-methylamino)-3-phenylpropanol

: 221134-15-2
(2S)-2--3-phenylpropyl (E)-3-pentenoate

Guidance literature:: With triethylamine; In tetrachloromethane; at 0 - 25 ℃; for 6.5h;
DOI:10.3987/COM-98-8298

Reference yield: 85.0%

: 221134-15-2
(2S)-2--3-phenylpropyl (E)-3-pentenoate

: 221134-33-4
N1-<(1S)-1-benzyl-2-hydroxyethyl>-N1-methyl-3-(E)-pentenamide

Guidance literature:: With potassium carbonate; In methanol;
DOI:10.3987/COM-98-8298

Reference yield:

: 221134-15-2
(2S)-2--3-phenylpropyl (E)-3-pentenoate

: 221134-49-2
N1-<(1S)-1-benzyl-2-oxoethyl>-N1-methyl-(E)-3-pentenamide

Guidance literature:: Multi-step reaction with 2 steps

1: 85 percent / 6 percent aq K₂CO₃ / methanol

2: 60 percent / DMSO, bis(trichloromethyl)carbonate, NEt₃ / CH₂Cl₂ / 2.5 h

With bis(trichloromethyl) carbonate; potassium carbonate; dimethyl sulfoxide; triethylamine; In methanol; dichloromethane;
DOI:10.3987/COM-98-8298