methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

Base Information

Chemical Name:methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate
CAS No.:145661-89-8
Molecular Formula:C₃₃H₃₀Cl₃NO₁₀
Molecular Weight:706.961
Hs Code.:

Synonyms:methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

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Technology Process of methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

There total 5 articles about methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114663-53-5,130506-36-4
(2S,3S,4S,5R,6S)-3,4,5-Triacetoxy-6-allyloxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 145661-89-8
methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

Guidance literature:: Multi-step reaction with 3 steps

1: NaOMe / methanol; tetrahydrofuran

2: pyridine

With pyridine; sodium methylate; In tetrahydrofuran; methanol;
DOI:10.1016/S0040-4039(00)61790-2

Reference yield:

: 7355-18-2
(2S,3S,4S,5R,6S)-3,4,5,6-Tetraacetoxy-tetrahydro-pyran-2-carboxylic acid methyl ester

: 145661-89-8
methyl (2,3,4-tri-O-4-methylbenzoyl-α-D-glucopyranosyl trichloroacetimidate)uronate

Guidance literature:: Multi-step reaction with 4 steps

1: SnCl₄ / 1,2-dichloro-ethane

2: NaOMe / methanol; tetrahydrofuran

3: pyridine

With pyridine; sodium methylate; tin(IV) chloride; In tetrahydrofuran; methanol; 1,2-dichloro-ethane;
DOI:10.1016/S0040-4039(00)61790-2