(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

Base Information

Chemical Name:(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate
CAS No.:1315571-42-6
Molecular Formula:C₇H₆O₄*C₂₁H₃₁N₇O
Molecular Weight:551.646
Hs Code.:

Synonyms:(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

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Chemical Property of (2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

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Technology Process of (2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

There total 3 articles about (2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 1070790-89-4
(2R,3S)-3-(6-((4,6-dimethylpyridin-3-ylmethyl)amino)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol

: 490-79-9
2,5-dihydroxybenzoic acid.

: 1315571-42-6
(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

Guidance literature:: In ethyl acetate; at 20 - 40 ℃; for 63h; Product distribution / selectivity;

Reference yield:

: 482615-48-5
(2R,3S)-3-amino-pentan-2-ol

: 1315571-42-6
(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / ethylene glycol / 125 °C / Inert atmosphere

2: ethyl acetate / 63 h / 20 - 40 °C

With N-ethyl-N,N-diisopropylamine; In ethylene glycol; ethyl acetate;

Reference yield:

: 1070791-10-4
(4,6-dimethylpyridin-3-ylmethyl)-(2-fluoro-9-isopropyl-9H-purin-6-yl)-amine

: 1315571-42-6
(2R,3S)-3-(6-(2-(4,6-dimethylpyridin-3-yl)ethyl)-9-isopropyl-9H-purin-2-ylamino)pentan-2-ol gentisate

Guidance literature:: Multi-step reaction with 2 steps

1: N-ethyl-N,N-diisopropylamine / ethylene glycol / 125 °C / Inert atmosphere

2: ethyl acetate / 63 h / 20 - 40 °C

With N-ethyl-N,N-diisopropylamine; In ethylene glycol; ethyl acetate;