methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

Base Information

Chemical Name:methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside
CAS No.:187218-18-4
Molecular Formula:C₂₁H₃₂Cl₂N₂O₆
Molecular Weight:479.401
Hs Code.:

Synonyms:methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

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Chemical Property of methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

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Technology Process of methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

There total 3 articles about methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 79.0%

: 68396-86-1,496811-81-5
methyl 6-deoxy-6-tert-butoxycarbonylamino-β-D-glucopyranoside

: 187218-20-8
4-{4-[bis(2-chloroethyl)amino]phenyl}butyric acid 4-nitrophenyl ester

: 187218-18-4
methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

Guidance literature:: With triethylamine; In ethanol; at 20 ℃; for 4h;
DOI:10.1016/S0014-2999(96)00796-0

Reference yield:

: 87586-16-1
(2R,3S,4S,5R,6R)-2-(azidomethyl)-6-methoxytetrahydro-2H-pyran-3,4,5-triol

: 187218-18-4
methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogen / palladium on carbon / ethanol / 1.5 h / 20 °C

2: 79 percent / triethylamine / ethanol / 4 h / 20 °C

With hydrogen; triethylamine; palladium on activated charcoal; In ethanol;
DOI:10.1016/S0014-2999(96)00796-0

Reference yield:

: 709-50-2
methyl beta-D-glucopyranoside

: 187218-18-4
methyl 6-{4-[bis(2-chloroethyl)amino]benzenebutanoylamido}-6-deoxy-β-D-glucopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 64 percent / triphenylphosphine; lithium azide; carbon tetrabromide / dimethylformamide / 22.5 h / 20 - 55 °C

2: hydrogen / palladium on carbon / ethanol / 1.5 h / 20 °C

3: 79 percent / triethylamine / ethanol / 4 h / 20 °C

With lithium azide; carbon tetrabromide; hydrogen; triethylamine; triphenylphosphine; palladium on activated charcoal; In ethanol; N,N-dimethyl-formamide;
DOI:10.1016/S0014-2999(96)00796-0