rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate

Base Information

• Chemical Name: rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate
• CAS No.: 82338-59-8
• Molecular Formula: C₄₁H₄₀As₄ClORu*F₆P
• Molecular Weight: 1129.94

Synonyms:rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate

Chemical Property of rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate

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Technology Process of rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate

There total 1 articles about rac-anti-cis-C₁-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

ammonium hexafluorophosphate + rac-anti-cis-C2-dichloro((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) (82442-76-0) → rac-anti-cis-C1-carbonylhydridobis((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II) hexafluorophosphate (82338-59-8)

Guidance literature:

With CO; In ethanol; CO passed into boiling suspn. of Ru complex and NH4PF6 in ethanol for 20 min, cooled to room temp., treated with water; CO stream stopped, ppt. filtered off, washed with water, dried, recrystd. from acetone by addn. of diethyl ether;

upstream raw materials:

rac-anti-cis-C₂-dichloro((RR,SS)-o-phenylenebis(methylphenylarsine))ruthenium(II)

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