2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine

Base Information

• Chemical Name: 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine
• CAS No.: 201855-39-2
• Molecular Formula: C₅₄H₄₆N₆O₁₂
• Molecular Weight: 970.992

Synonyms:2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine

Chemical Property of 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine

Chemical Property:

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Technology Process of 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine

There total 1 articles about 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

benzoyl cyanide (613-90-1) + 5'-O-(dimethoxytrityl)-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine (156046-12-7) → 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine (201855-39-2)

Guidance literature:

With tributyl-amine; In acetonitrile; for 2h; Ambient temperature;

DOI:10.1002/hlca.19980810106

Reference yield: 95.0%

2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine (201855-39-2) → 2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)adenosine (201855-40-5)

Guidance literature:

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine; for 18h;

DOI:10.1002/hlca.19980810106

Reference yield:

2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)-N6-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine (201855-39-2) → 2',3'-di-O-benzoyl-N6,N6-[2-(2-carboxyethyl)glutaryl]-5'-O-(4,4'-dimethoxytrityl)adenosine

Guidance literature:

Multi-step reaction with 2 steps

1: 95 percent / DBU / pyridine / 18 h

2: 80 percent / pyridine / 6 h / 90 °C

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In pyridine;

DOI:10.1002/hlca.19980810106

upstream raw materials:

benzoyl cyanide

5'-O-(dimethoxytrityl)-N⁶-[2-(4-nitrophenyl)ethoxycarbonyl]adenosine

Downstream raw materials:

2',3'-di-O-benzoyl-5'-O-(4,4'-dimethoxytrityl)adenosine

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