(-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde

Base Information

• Chemical Name: (-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde
• CAS No.: 1033126-33-8
• Molecular Formula: C₃₂H₄₀O₆Si
• Molecular Weight: 548.751

Synonyms:(-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde

Chemical Property of (-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde

Chemical Property:

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Technology Process of (-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde

There total 1 articles about (-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

C33H42O5Si (1033126-70-3) → (-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde (1033126-33-8)

Guidance literature:

C₃₃H₄₂O₅Si; With ozone; In methanol; dichloromethane; at -78 ℃;

With dimethylsulfide; In methanol; dichloromethane; at -78 - 20 ℃; Further stages.;

DOI:10.1021/jo8004233

Reference yield: 80.0%

(-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde (1033126-33-8) + 2,2-dimethylpent-4-enyl iodide (95106-80-2) → C39H54O6Si (1033126-34-9)

Guidance literature:

2,2-dimethylpent-4-enyl iodide; With tert.-butyl lithium; In pentane; at -55 ℃; for 1h;

(-)-(1R,2S,3R)-3-(4-methoxybenzyloxy)-1-(tert-butyldiphenylsiloxymethyl)-2-(methoxymethoxy)cyclobutanecarbaldehyde; In tetrahydrofuran; pentane; at -55 - -40 ℃; Further stages.;

DOI:10.1021/jo8004233

upstream raw materials:

C₃₃H₄₂O₅Si

Downstream raw materials:

C₃₉H₅₄O₆Si

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