dicyclohexylmethoxyallyl ether

Base Information

Chemical Name:dicyclohexylmethoxyallyl ether
CAS No.:442533-05-3
Molecular Formula:C₁₆H₂₈O
Molecular Weight:236.398
Hs Code.:

Synonyms:dicyclohexylmethoxyallyl ether

Suppliers and Price of dicyclohexylmethoxyallyl ether

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of dicyclohexylmethoxyallyl ether

Chemical Property:

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Technology Process of dicyclohexylmethoxyallyl ether

There total 1 articles about dicyclohexylmethoxyallyl ether which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 71.0%

: 4453-82-1
Dicyclohexylmethanol

: 106-95-6
allyl bromide

: 442533-05-3
dicyclohexylmethoxyallyl ether

Guidance literature:: Dicyclohexylmethanol; With sodium hydride; In tetrahydrofuran; for 1h; Heating;

allyl bromide; In tetrahydrofuran; for 15h; Further stages.; Heating;
DOI:10.1021/ja020446a

Reference yield: 82.0%

: 442533-05-3
dicyclohexylmethoxyallyl ether

: 442533-06-4
3-(dicyclohexylmethyl)oxypropan-1-ol

Guidance literature:: dicyclohexylmethoxyallyl ether; With borane-THF; at 20 ℃; for 0.5h;

With sodium hydroxide; dihydrogen peroxide; at 50 ℃; for 1h; Further stages.;
DOI:10.1021/ja020446a

Reference yield:

: 442533-05-3
dicyclohexylmethoxyallyl ether

: N-[3-(dicyclohexylmethyl)oxypropyl]-N'-methyl-4,4-bipyridinium iodide salt

Guidance literature:: Multi-step reaction with 3 steps

1.1: BH₃*THF / 0.5 h / 20 °C

1.2: 82 percent / aq. NaOH; H₂O₂ / 1 h / 50 °C

2.1: 89 percent / (PhO)3P; MeI / 48 h / 130 °C

3.1: acetonitrile / 48 h / Heating

With triphenyl phosphite; borane-THF; methyl iodide; In acetonitrile;
DOI:10.1021/ja020446a