methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

Base Information

Chemical Name:methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside
CAS No.:213829-05-1
Molecular Formula:C₄₁H₄₀O₁₃
Molecular Weight:740.761
Hs Code.:

Synonyms:methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

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Chemical Property of methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

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Technology Process of methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

There total 2 articles about methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 42.0%

: 213829-02-8
methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-3-O-benzyl-2,4-dideoxy-2,4-diiodo-α-D-galactopyranoside

: 213829-05-1
methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

Guidance literature:: With hydrogen; sodium hydrogencarbonate; palladium on activated charcoal; In methanol; water; ethyl acetate; for 4h; under 5171.5 Torr;
DOI:10.1016/S0008-6215(98)00107-4

Reference yield:

: 174089-82-8
methyl 3-O-benzyl-2-deoxy-2-iodo-6-O-(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-α-D-mannopyranoside

: 213829-05-1
methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / triphenylphosphine, triiodoimidazole / toluene / 110 °C

2: 42 percent / H₂, NaHCO₃ / 10percent Pd-C / ethyl acetate; methanol; H₂O / 4 h / 5171.5 Torr

With tri-iodoimidazole; hydrogen; sodium hydrogencarbonate; triphenylphosphine; palladium on activated charcoal; In methanol; water; ethyl acetate; toluene;
DOI:10.1016/S0008-6215(98)00107-4

Reference yield: 65.0%

: 2,4,6-tri-O-benzoyl-3-deoxy-α-D-arabino-hexopyranosyl chloride

: 213829-05-1
methyl (2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)-2,4-dideoxy-α-D-threo-hexopyranoside

: methyl (2,4,6-tri-O-benzoyl-3-deoxy-α-D-arabino-hexopyranosyl)-(1->3)-[(2,3,4,6-tetra-O-benzoyl-α-D-mannopyranosyl)-(1->6)]-2,4-dideoxy-α-D-threo-hexopyranoside

Guidance literature:: With 2,6-di-tert-butyl-pyridine; 4 A molecular sieve; silver trifluoromethanesulfonate; In dichloromethane; toluene; at -20 ℃; for 1.5h;
DOI:10.1016/S0008-6215(98)00107-4