(S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one

Base Information

• Chemical Name: (S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one
• CAS No.: 231609-87-3
• Molecular Formula: C₂₅H₃₆N₂O₄S
• Molecular Weight: 460.638

Synonyms:(S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one

Chemical Property of (S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one

Chemical Property:

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Technology Process of (S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one

There total 1 articles about (S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ⁶-thia-4-aza-tricyclo[5.2.1.0^1,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

(E)-1-bromo-4-methyl-2-pentene (66222-05-7) + ((1S,5R,7R)-10,10-Dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-oxo-acetaldehyde O-benzyl-oxime → (S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one (231609-87-3)

Guidance literature:

With ammonium chloride; zinc; In tetrahydrofuran;

DOI:10.1016/S0960-894X(99)00218-8

Reference yield: 80.0%

(S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one (231609-87-3) → (S)-2-Benzyloxyamino-3-isopropyl-pent-4-enoic acid

Guidance literature:

With lithium hydroxide; In tetrahydrofuran;

DOI:10.1016/S0960-894X(99)00218-8

Reference yield:

(S)-2-Benzyloxyamino-1-((1S,5R,7R)-10,10-dimethyl-3,3-dioxo-3λ6-thia-4-aza-tricyclo[5.2.1.01,5]dec-4-yl)-3-isopropyl-pent-4-en-1-one (231609-87-3) → 2-benzyloxyamino-3-isopropyl-pent-4-enoic acid tert-butyl ester

Guidance literature:

Multi-step reaction with 2 steps

1: 80 percent / aq. LiOH / tetrahydrofuran

With lithium hydroxide; In tetrahydrofuran;

DOI:10.1016/S0960-894X(99)00218-8

upstream raw materials:

(E)-1-bromo-4-methyl-2-pentene

Downstream raw materials:

C₂₇H₃₅NO₅

C₂₇H₃₇NO₈S

C₂₇H₃₇NO₈S

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