(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Base Information

Chemical Name:(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure
CAS No.:95853-80-8
Molecular Formula:C₁₅H₂₃NO₄
Molecular Weight:281.352
Hs Code.:

Synonyms:(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Suppliers and Price of (2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

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Chemical Property of (2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

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Technology Process of (2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

There total 3 articles about (2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 95853-79-5
(2S)-(+)-2-<(4S,5S)-(2,2-Dimethyl-4-phenyl-1,3-dioxan-5-yl)amino>-4-methylvaleronitril

: 95853-80-8
(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Guidance literature:: With hydrogenchloride; In water; 1.) 1 h, -13 deg C, 2.) 1h, 0 deg C, 3.) 1 h, room temperature, 4.) 4 h, 60 deg C;

Reference yield:

: 590-86-3
isovaleraldehyde

: 95853-80-8
(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / ethane-1,2-diol / 1 h / Ambient temperature

2: 78 percent / 12 N HCl / H₂O / 1.) 1 h, -13 deg C, 2.) 1h, 0 deg C, 3.) 1 h, room temperature, 4.) 4 h, 60 deg C

With hydrogenchloride; In water; ethylene glycol;

Reference yield:

: 35019-66-0
(4S,5S)-2,2-dimethyl-4-phenyl-1,3-dioxan-5-amine

: 95853-80-8
(2S)-(+)-2-<(1S,2S)-(2-Hydroxy-1-hydroxymethyl-2-phenylethyl)amino>-4-methylvaleriansaeure

Guidance literature:: Multi-step reaction with 2 steps

1: 40 percent / ethane-1,2-diol / 1 h / Ambient temperature

2: 78 percent / 12 N HCl / H₂O / 1.) 1 h, -13 deg C, 2.) 1h, 0 deg C, 3.) 1 h, room temperature, 4.) 4 h, 60 deg C

With hydrogenchloride; In water; ethylene glycol;