diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

Base Information

Chemical Name:diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane
CAS No.:887602-19-9
Molecular Formula:C₂₃H₃₆O₃Si
Molecular Weight:388.623
Hs Code.:

Synonyms:diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

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Chemical Property of diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

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Technology Process of diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

There total 4 articles about diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 82.0%

: 887602-35-9
(2S,3S)-3-(Diisopropyl-prop-1-ynyl-silanyloxy)-2-methyl-pent-4-en-1-ol

: 89238-99-3
O-(4-methoxybenzyl)-trichloroacetimidate

: 887602-19-9
diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

Guidance literature:: With camphor-10-sulfonic acid; In dichloromethane; at -10 - 20 ℃;
DOI:10.1021/ja0609708

Reference yield:

: 321921-73-7
(4R,2'R,3'S)-4-benzyl-3-[3-hydroxy-2-methylpent-4-enoyl]-oxazolidin-2-one

: 887602-19-9
diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

Guidance literature:: Multi-step reaction with 3 steps

1: 97 percent / imidazole / dimethylformamide / 1 h / 20 °C

2: 78 percent / LiBH₄ / tetrahydrofuran / 6 h / 0 °C

3: 82 percent / CSA / CH₂Cl₂ / -10 - 20 °C

With 1H-imidazole; lithium borohydride; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1021/ja0609708

Reference yield:

: 887602-34-8
(R)-4-Benzyl-3-[(2R,3S)-3-(diisopropyl-prop-1-ynyl-silanyloxy)-2-methyl-pent-4-enoyl]-oxazolidin-2-one

: 887602-19-9
diisopropyl-{1-[2-(4-methoxy-benzyloxy)-1-methyl-ethyl]-allyloxy}-prop-1-ynyl-silane

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / LiBH₄ / tetrahydrofuran / 6 h / 0 °C

2: 82 percent / CSA / CH₂Cl₂ / -10 - 20 °C

With lithium borohydride; camphor-10-sulfonic acid; In tetrahydrofuran; dichloromethane;
DOI:10.1021/ja0609708