(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

Base Information

Chemical Name:(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane
CAS No.:183209-10-1
Molecular Formula:C₂₅H₃₀O₃
Molecular Weight:378.511
Hs Code.:

Synonyms:(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

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Technology Process of (+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

There total 5 articles about (+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 183209-09-8
(+/-)-7-(3-cyano-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

: 183209-10-1
(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

Guidance literature:: With diisobutylaluminium hydride; In hexane; dichloromethane; -20 deg C, 30 min; -20 deg C -> 20 deg C, 2.5 h;
DOI:10.1080/00397919608003828

Reference yield:

: 68269-56-7,54735-44-3
3-methyl-3-vinylcyclohexan-1-one

: 183209-10-1
(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

Guidance literature:: Multi-step reaction with 5 steps

1: 83 percent / HBr(gas) / hexane / Irradiation

2: 89 percent / NaI / acetone / 24 h / Heating

3: 98 percent / p-TsOH / benzene / 12 h / Heating

4: 81 percent / KOH / butan-2-one / 24 h / Heating

5: 95 percent / DIBAL-H / CH₂Cl₂; hexane / -20 deg C, 30 min; -20 deg C -> 20 deg C, 2.5 h

With potassium hydroxide; hydrogen bromide; diisobutylaluminium hydride; toluene-4-sulfonic acid; sodium iodide; In hexane; dichloromethane; acetone; butanone; benzene;
DOI:10.1080/00397919608003828

Reference yield:

: 183209-08-7
(+/-)-7-(2-iodoethyl)-7-methyl-1,4-dioxaspiro[4.5]decane

: 183209-10-1
(+/-)-7-(3-formyl-3,3-diphenylpropyl)-7-methyl-1,4-dioxaspiro[4.5]decane

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / KOH / butan-2-one / 24 h / Heating

2: 95 percent / DIBAL-H / CH₂Cl₂; hexane / -20 deg C, 30 min; -20 deg C -> 20 deg C, 2.5 h

With potassium hydroxide; diisobutylaluminium hydride; In hexane; dichloromethane; butanone;
DOI:10.1080/00397919608003828