4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione

Base Information

• Chemical Name: 4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione
• CAS No.: 102423-44-9
• Molecular Formula: C₁₂H₁₄N₄S₂
• Molecular Weight: 278.402

Synonyms:4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione

Chemical Property of 4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione

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Technology Process of 4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione

There total 1 articles about 4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

4-methyl-benzaldehyde (104-87-0) + 4-amino-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione (86672-63-1) → 4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione (102423-44-9)

Guidance literature:

With hydrogenchloride; In methanol; for 0.5h; Heating;

Reference yield: 79.0%

4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione (102423-44-9) + para-bromophenacyl bromide (99-73-0,132309-76-3) → (6S,7R)-7-(4-Bromo-benzoyl)-1-methyl-3-methylsulfanyl-6-p-tolyl-6,7-dihydro-5H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-1-ium; bromide (113385-45-8,113385-55-0)

Guidance literature:

In methanol; for 20h; Heating;

Reference yield: 52.0%

4-<(4-methylbenzylidene)amino>-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione (102423-44-9) → 1-methyl-6-(4-methylphenyl)-3-(methylthio)-1,2,4-triazolo<3,4-b><1,3,4>thiadiazolium chloride (102423-54-1)

Guidance literature:

With phosphorus pentachloride; In toluene; for 16h; Heating;

upstream raw materials:

4-methyl-benzaldehyde

4-amino-2,4-dihydro-2-methyl-5-(methylthio)-3H-1,2,4-triazole-3-thione

Downstream raw materials:

1-methyl-3-methylthio-6-phenyl-7H-1,2,4-triazolo<3,4-b><1,3,4>thiadiazinium chloride

1-methyl-6-(4-methylphenyl)-3-(methylthio)-1,2,4-triazolo<3,4-b><1,3,4>thiadiazolium chloride

(6S,7R)-7-(4-Bromo-benzoyl)-1-methyl-3-methylsulfanyl-6-p-tolyl-6,7-dihydro-5H-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazin-1-ium; bromide

C₂₀H₁₉BrN₄OS₂

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