Technology Process of C20H36O4Si
There total 7 articles about C20H36O4Si which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
tetra-(n-butyl)ammonium iodide; sodium hydride;
In
N,N,N,N,N,N-hexamethylphosphoric triamide;
at -15 ℃;
for 3h;
DOI:10.1016/j.tetlet.2011.12.015
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
2: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide;
1: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015
- Guidance literature:
-
Multi-step reaction with 3 steps
1: oxygen; palladium diacetate / dimethyl sulfoxide / 72 h / 55 °C
2: sodium tetrahydroborate; cerium(III) chloride heptahydrate / methanol / 0.25 h
3: tetra-(n-butyl)ammonium iodide; sodium hydride / N,N,N,N,N,N-hexamethylphosphoric triamide / 3 h / -15 °C
With
sodium tetrahydroborate; cerium(III) chloride heptahydrate; oxygen; palladium diacetate; tetra-(n-butyl)ammonium iodide; sodium hydride;
In
methanol; N,N,N,N,N,N-hexamethylphosphoric triamide; dimethyl sulfoxide;
2: Luche reduction;
DOI:10.1016/j.tetlet.2011.12.015
