(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

Base Information

Chemical Name:(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane
CAS No.:79357-09-8
Molecular Formula:C₁₂H₂₁NO₂S
Molecular Weight:243.37
Hs Code.:

Synonyms:(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

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Chemical Property of (1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

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Technology Process of (1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

There total 5 articles about (1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 79357-08-7
(-)-N-<(neomenthylsulfonyl)methyl>formamide

: 79357-09-8
(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

Guidance literature:: With triethylamine; trichlorophosphate; at 0 ℃; for 0.5h;
DOI:10.1021/jo00338a019

Reference yield:

: 53273-24-8,196622-67-0,223653-15-4,173006-99-0
(1S,2S,5R)-(+)-neomenthyl thiol

: 79357-09-8
(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

Guidance literature:: Multi-step reaction with 3 steps

1: 1) t-BuOK / 1) ether, DMSO, rt, 1h, 2) rt, 5 h

2: 95 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / Ambient temperature

3: 73 percent / POCl₃, Et₃N / 0.5 h / 0 °C

With potassium tert-butylate; triethylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In dichloromethane;
DOI:10.1021/jo00338a019

Reference yield:

: 79357-07-6
(+)-N-<(neomenthylthio)methyl>formamide

: 79357-09-8
(1S,2S,4R)-2-((isocyanomethyl)sulfonyl)-4-methyl-1-isopropylcyclohexane

Guidance literature:: Multi-step reaction with 2 steps

1: 95 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / Ambient temperature

2: 73 percent / POCl₃, Et₃N / 0.5 h / 0 °C

With triethylamine; 3-chloro-benzenecarboperoxoic acid; trichlorophosphate; In dichloromethane;
DOI:10.1021/jo00338a019