ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

Base Information

Chemical Name:ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate
CAS No.:808743-50-2
Molecular Formula:C₂₁H₂₄Cl₂N₂O₄
Molecular Weight:439.339
Hs Code.:

Synonyms:ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

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Chemical Property of ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

Chemical Property:

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Technology Process of ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

There total 5 articles about ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 808743-49-9
ethyl 4-[4-(acetylamino)-3-aminophenoxy]butanoate hydrochloride

: 94-99-5
2,4-Dichlorobenzyl chloride

: 808743-50-2
ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

Guidance literature:: With potassium carbonate; In DMF (N,N-dimethyl-formamide); at 20 - 90 ℃; for 4h;

Reference yield:

: 808744-15-2
ethyl 4-[4-(acetylamino)-3-nitrophenoxy]butanoate

: 808743-50-2
ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

Guidance literature:: Multi-step reaction with 3 steps

1: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 3 h / 20 °C / 760.05 Torr

2: hydrogenchloride / 1,4-dioxane; ethanol / 0.5 h / 20 °C

3: potassium carbonate / DMF (N,N-dimethyl-formamide) / 4 h / 20 - 90 °C

With hydrogenchloride; hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; DMF (N,N-dimethyl-formamide); ethanol;

Reference yield:

: 2969-81-5
Ethyl 4-bromobutyrate

: 808743-50-2
ethyl 4-{4-(acetylamino)-3-[(2,4-dichlorobenzyl)amino]phenoxy}butanoate

Guidance literature:: Multi-step reaction with 4 steps

1: potassium carbonate / DMF (N,N-dimethyl-formamide) / 48 h / 20 °C

2: hydrogen / palladium 10% on activated carbon / tetrahydrofuran; ethanol / 3 h / 20 °C / 760.05 Torr

3: hydrogenchloride / 1,4-dioxane; ethanol / 0.5 h / 20 °C

4: potassium carbonate / DMF (N,N-dimethyl-formamide) / 4 h / 20 - 90 °C

With hydrogenchloride; hydrogen; potassium carbonate; palladium 10% on activated carbon; In tetrahydrofuran; 1,4-dioxane; DMF (N,N-dimethyl-formamide); ethanol;