Technology Process of C20H25NO6S
There total 3 articles about C20H25NO6S which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
manganese(IV) oxide; copper(II) bis(trifluoromethanesulfonate); (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole);
In
chloroform;
at 20 ℃;
for 24h;
enantioselective reaction;
Inert atmosphere;
DOI:10.1021/ja309311z
- Guidance literature:
-
Multi-step reaction with 3 steps
1: dichloromethane / 24 h / Inert atmosphere; Reflux
2: magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere
3: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); copper(II) bis(trifluoromethanesulfonate); manganese(IV) oxide / chloroform / 24 h / 20 °C / Inert atmosphere
With
manganese(IV) oxide; copper(II) bis(trifluoromethanesulfonate); magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole);
In
dichloromethane; chloroform;
DOI:10.1021/ja309311z
- Guidance literature:
-
Multi-step reaction with 2 steps
1: magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine / dichloromethane / 20 °C / Inert atmosphere
2: (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole); copper(II) bis(trifluoromethanesulfonate); manganese(IV) oxide / chloroform / 24 h / 20 °C / Inert atmosphere
With
manganese(IV) oxide; copper(II) bis(trifluoromethanesulfonate); magnesium bromide ethyl etherate; N-ethyl-N,N-diisopropylamine; (4R,4'R)-2,2'-(propane-2,2'diyl)bis(4-phenyl-4,5-dihydrooxazole);
In
dichloromethane; chloroform;
DOI:10.1021/ja309311z