[3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester

Base Information

• Chemical Name: [3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester
• CAS No.: 892413-78-4
• Molecular Formula: C₁₅H₂₄N₂O₄
• Molecular Weight: 296.367

Synonyms:[3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester

Chemical Property of [3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester

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Technology Process of [3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester

There total 1 articles about [3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

tert-butyl (3-(2-methoxy-5-nitrophenoxy)propyl)carbamate (892413-77-3) → [3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester (892413-78-4)

Guidance literature:

With hydrogen; Raney Nickel; In methanol; at 20 ℃; for 2h; under 2250.23 Torr;

Reference yield: 53.2%

[3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester (892413-78-4) + C14H19ClN4O2 (1111235-64-3) → C29H42N6O6 (1111235-68-7)

Guidance literature:

[3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester; C₁₄H₁₉ClN₄O₂; With hydrogenchloride; In 1,4-dioxane; acetonitrile; at 75 ℃; for 3h;

With ammonium bicarbonate; In water; acetonitrile;

Reference yield: 41.0%

[3-(5-amino-2-methoxyphenoxy)propyl]-carbamic acid 1,1-dimethylethyl ester (892413-78-4) + N-[(4-chloro-2-[(6-iodo-4-pyrimidinyl)amino]phenyl)acetyl]-L-leucine 1,1-dimethylethyl ester (892413-90-0) → N-[[4-chloro-2-[[6-[[3-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-4-methoxyphenyl]amino]-4-pyrimidinyl]amino]phenyl]acetyl]-L-leucine 1,1-dimethylethyl ester (892413-91-1)

Guidance literature:

With hydrogenchloride; In isopropyl alcohol; tert-butyl alcohol; for 18h; Heating / reflux;

upstream raw materials:

tert-butyl (3-(2-methoxy-5-nitrophenoxy)propyl)carbamate

Downstream raw materials:

N-[[4-chloro-2-[[6-[[3-[3-[[(1,1-dimethylethoxy)carbonyl]amino]propoxy]-4-methoxyphenyl]amino]-4-pyrimidinyl]amino]phenyl]acetyl]-L-leucine 1,1-dimethylethyl ester

C₂₉H₄₂N₆O₆

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