Technology Process of C17H26O9
There total 6 articles about C17H26O9 which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
20 % Pd(OH)2/C;
In
methanol;
at 23 ℃;
for 2.25h;
under 760.051 Torr;
Inert atmosphere;
DOI:10.1021/ja206339s
- Guidance literature:
-
Multi-step reaction with 5 steps
1: dihydrogen peroxide; potassium hydroxide / methanol; water / 1.5 h / 65 °C / Inert atmosphere
2: tris-(dibenzylideneacetone)dipalladium(0); potassium hydroxide; tert-butyl XPhos / 1,4-dioxane; water / 15 h / 80 °C / Inert atmosphere
3: potassium carbonate / N,N-dimethyl-formamide / 18 h / 0 - 23 °C / Inert atmosphere
4: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
5: 20 % Pd(OH)2/C / methanol / 2.25 h / 23 °C / 760.05 Torr / Inert atmosphere
With
tris-(dibenzylideneacetone)dipalladium(0); di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; dihydrogen peroxide; potassium carbonate; triphenylphosphine; potassium hydroxide; tert-butyl XPhos;
In
tetrahydrofuran; 1,4-dioxane; methanol; water; N,N-dimethyl-formamide;
DOI:10.1021/ja206339s
- Guidance literature:
-
Multi-step reaction with 2 steps
1: di-isopropyl azodicarboxylate; triphenylphosphine / tetrahydrofuran / 18 h / 23 °C / Inert atmosphere
2: 20 % Pd(OH)2/C / methanol / 2.25 h / 23 °C / 760.05 Torr / Inert atmosphere
With
di-isopropyl azodicarboxylate; 20 % Pd(OH)2/C; triphenylphosphine;
In
tetrahydrofuran; methanol;
DOI:10.1021/ja206339s
