N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Base Information

Chemical Name:N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide
CAS No.:1574475-13-0
Molecular Formula:C₁₈H₁₉NO₂
Molecular Weight:281.354
Hs Code.:

Synonyms:N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Suppliers and Price of N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Chemical Property:

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Technology Process of N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

There total 12 articles about N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₆H₁₇NO

: 108-24-7
acetic anhydride

: 1574475-13-0
N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Guidance literature:: With dmap; triethylamine; In dichloromethane; at 0 - 20 ℃;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 1574475-15-2
(R)-N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)tert-butylsulfinamide

: 1574475-13-0
N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride / methanol / 20 °C

2: dmap; triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; dmap; triethylamine; In methanol; dichloromethane;
DOI:10.1080/00397911.2013.841938

Reference yield:

: 1574474-97-7
(R)-tert-butanesulfinylaldimine

: 1574475-13-0
N-((1S,2R)-2-hydroxy-2-phenyl-1,2,3,4-tetrahydronaphthalen-1-yl)acetamide

Guidance literature:: Multi-step reaction with 3 steps

1: samarium diiodide / tetrahydrofuran / 3 h / 20 °C / Inert atmosphere

2: hydrogenchloride / methanol / 20 °C

3: dmap; triethylamine / dichloromethane / 0 - 20 °C

With hydrogenchloride; dmap; samarium diiodide; triethylamine; In tetrahydrofuran; methanol; dichloromethane;
DOI:10.1080/00397911.2013.841938