Technology Process of C22H22F6N2O2
There total 6 articles about C22H22F6N2O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
potassium carbonate;
In
methanol;
for 0.5h;
- Guidance literature:
-
Multi-step reaction with 6 steps
1.1: diethyl ether; dichloromethane / 3 h / -78 °C
2.1: ozone / dichloromethane / 0.17 h / -78 °C
2.2: Inert atmosphere
3.1: caesium carbonate / N,N-dimethyl-formamide / 3 h / 23 °C
4.1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / Inert atmosphere
5.1: hydrogenchloride / methanol; 1,4-dioxane / 3.5 h / 0 - 23 °C
6.1: potassium carbonate / methanol / 0.5 h
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate; caesium carbonate; ozone;
In
1,4-dioxane; methanol; diethyl ether; ethanol; dichloromethane; N,N-dimethyl-formamide;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: palladium 10% on activated carbon; hydrogen / ethanol / 24 h / Inert atmosphere
2: hydrogenchloride / methanol; 1,4-dioxane / 3.5 h / 0 - 23 °C
3: potassium carbonate / methanol / 0.5 h
With
hydrogenchloride; palladium 10% on activated carbon; hydrogen; potassium carbonate;
In
1,4-dioxane; methanol; ethanol;