Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel-

Base Information

Chemical Name:Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel-
CAS No.:102675-62-7
Molecular Formula:C₁₁H₁₇NO₂
Molecular Weight:195.261
Hs Code.:

Synonyms:Benzenemethanol, 4-methoxy-a-[1-(methylamino)ethyl]-, (R*,S*)- (9CI); Benzenemethanol,4-methoxy-a-[1-(methylamino)ethyl]-, (R*,S*)-(?à)-;dl-4-Methoxyephedrine

Suppliers and Price of Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Chemicals and raw materials
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Total 14 raw suppliers

Chemical Property of Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel-

Chemical Property:

Purity/Quality:: 99% ,98%,Electron Grade , ^*data from raw suppliers

Safty Information:

Pictogram(s):
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Technology Process of Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel-

There total 5 articles about Benzenemethanol, 4-methoxy-a-[(1R)-1-(methylamino)ethyl]-, (aS)-rel- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 21086-33-9
2-bromo-1-(4-methoxyphenyl)-1-propanone

: 102675-62-7,102734-77-0,102734-78-1,107911-54-6,107911-56-8
threo 1-(p-methoxyphenyl)-2-(N-methylamino)-1-propanol

Guidance literature:: Multi-step reaction with 4 steps

1: KI / acetone / 72 h / Ambient temperature

2: LiAlH₄ / diethyl ether / 1 h / Heating

3: H₂, HCl conc. / 10percent Pd/C / ethanol / 760 Torr

4: NaOH dil. / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; potassium iodide; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane; acetone;
DOI:10.1016/S0040-4020(01)87629-8

Reference yield:

: 101718-50-7
p-methoxy-(N-methyl benzylamino)-propiophenone

: 102675-62-7,102734-77-0,102734-78-1,107911-54-6,107911-56-8
threo 1-(p-methoxyphenyl)-2-(N-methylamino)-1-propanol

Guidance literature:: Multi-step reaction with 3 steps

1: LiAlH₄ / diethyl ether / 1 h / Heating

2: H₂, HCl conc. / 10percent Pd/C / ethanol / 760 Torr

3: NaOH dil. / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; lithium aluminium tetrahydride; hydrogen; palladium on activated charcoal; In diethyl ether; ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)87629-8

Reference yield:

: 107841-25-8
threo 1-(p-methoxyphenyl)-2-(N-methylbenzylamino)-1-propanol

: 102675-62-7,102734-77-0,102734-78-1,107911-54-6,107911-56-8
threo 1-(p-methoxyphenyl)-2-(N-methylamino)-1-propanol

Guidance literature:: Multi-step reaction with 2 steps

1: H₂, HCl conc. / 10percent Pd/C / ethanol / 760 Torr

2: NaOH dil. / CH₂Cl₂

With hydrogenchloride; sodium hydroxide; hydrogen; palladium on activated charcoal; In ethanol; dichloromethane;
DOI:10.1016/S0040-4020(01)87629-8