N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide

Base Information

• Chemical Name: N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide
• CAS No.: 942212-27-3
• Molecular Formula: C₂₂H₁₇BrN₂O₃
• Molecular Weight: 437.293

Synonyms:N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide

Chemical Property of N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide

Chemical Property:

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Technology Process of N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide

There total 1 articles about N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C22H19BrN2O4 (1208916-20-4) → N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide (942212-27-3)

Guidance literature:

C₂₂H₁₉BrN₂O₄; pyridinium p-toluenesulfonate; In o-xylene; Heating / reflux;

With sodium hydrogencarbonate; In o-xylene; water; ethyl acetate;

Reference yield: 13.0%

N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide (942212-27-3) + tri-n-butyl(vinyl)tin (7486-35-3) → 2-(2-methylphenoxy)-N-[4-(5-vinyl-1,3-benzoxazol-2-yl)phenyl]acetamide

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; In N,N-dimethyl-formamide; at 80 ℃; for 12h;

DOI:10.1016/j.bmcl.2009.10.099

Reference yield:

N-[4-(5-bromo-1,3-benzoxazol-2-yl)phenyl]-2-(2-methylphenoxy)acetamide (942212-27-3) + trimethylsilylacetylene (1066-54-2) → C27H26N2O3Si

Guidance literature:

With diethylamine; bis-triphenylphosphine-palladium(II) chloride; copper(l) iodide; triphenylphosphine; In N,N-dimethyl-formamide; at 120 ℃; for 1.25h; Microwave irradiation;

upstream raw materials:

C₂₂H₁₉BrN₂O₄

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