C₃₈H₄₉NO₅Si₂

Base Information

Chemical Name:C₃₈H₄₉NO₅Si₂
CAS No.:1295471-06-5
Molecular Formula:C₃₈H₄₉NO₅Si₂
Molecular Weight:655.982
Hs Code.:

C<sub>38</sub>H<sub>49</sub>NO<sub>5</sub>Si<sub>2</sub>

Synonyms:C₃₈H₄₉NO₅Si₂

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Chemical Property of C₃₈H₄₉NO₅Si₂

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Technology Process of C₃₈H₄₉NO₅Si₂

There total 6 articles about C₃₈H₄₉NO₅Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 1295471-04-3
C₃₈H₅₁NO₆Si₂

: 1295471-06-5
C₃₈H₄₉NO₅Si₂

Guidance literature:: With pyridine; trifluoroacetyl chloride; In dichloromethane; at 20 ℃; for 8h;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-52-1
C₃₉H₅₅NO₅Si₂

: 1295471-06-5
C₃₈H₄₉NO₅Si₂

Guidance literature:: Multi-step reaction with 4 steps

1.1: oxalyl dichloride; dimethyl sulfoxide / dichloromethane / 0.5 h / -78 °C / Inert atmosphere

1.2: 1 h / -78 - 0 °C

2.1: ozone / dichloromethane / -78 °C

2.2: -78 - 20 °C

3.1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

4.1: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

With pyridine; chloro-trimethyl-silane; oxalyl dichloride; titanium tetrachloride; ozone; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; trifluoroacetyl chloride; In dichloromethane;
DOI:10.1002/anie.201008079

Reference yield:

: 1295471-53-2
C₃₈H₅₁NO₆Si₂

: 1295471-06-5
C₃₈H₄₉NO₅Si₂

Guidance literature:: Multi-step reaction with 2 steps

1: chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine / dichloromethane / 0.33 h / 0 °C

2: pyridine; trifluoroacetyl chloride / dichloromethane / 8 h / 20 °C

With pyridine; chloro-trimethyl-silane; titanium tetrachloride; N-ethyl-N,N-diisopropylamine; trifluoroacetyl chloride; In dichloromethane;
DOI:10.1002/anie.201008079