1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene

Base Information

• Chemical Name: 1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene
• CAS No.: 1159498-11-9
• Molecular Formula: C₂₆H₃₄Br₂N₂O₈
• Molecular Weight: 662.373

Synonyms:1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene

Chemical Property of 1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene

Chemical Property:

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Technology Process of 1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene

There total 1 articles about 1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.0%

1,10-bis(4,5-dimethoxy-2-nitrophenyl)-1,10-decanediol (1159498-06-2) → 1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene (1159498-11-9)

Guidance literature:

With Acetyl bromide; hydrogen bromide; at 0 - 20 ℃; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.03.009

Reference yield: 90.0%

1-[1,10-dibromo-10-(4,5-dimethoxy-2-nitrophenyl)decyl]-4,5-dimethoxy-2-nitro-benzene (1159498-11-9) + N-benzoyl-L-cysteine dimethyl ester (5673-89-2) → 2-(benzoylamino)-3-[[10[[(2R)-2-(benzoylamino)-3-methoxy-3-oxopropyl]thio]-1,10-bis(4,5-dimethoxy-2-nitrophenyl)decyl]thio]-(2R)-propanoic acid methyl ester (1159498-17-5)

Guidance literature:

With sodium hydrogencarbonate; In methanol; Inert atmosphere;

DOI:10.1016/j.tetlet.2009.03.009

upstream raw materials:

1,10-bis(4,5-dimethoxy-2-nitrophenyl)-1,10-decanediol

Downstream raw materials:

2-(benzoylamino)-3-[[10[[(2R)-2-(benzoylamino)-3-methoxy-3-oxopropyl]thio]-1,10-bis(4,5-dimethoxy-2-nitrophenyl)decyl]thio]-(2R)-propanoic acid methyl ester

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