C₁₅H₁₂BrF₆N₃O₂

Base Information

Chemical Name:C₁₅H₁₂BrF₆N₃O₂
CAS No.:1400917-00-1
Molecular Formula:C₁₅H₁₂BrF₆N₃O₂
Molecular Weight:460.174
Hs Code.:

C<sub>15</sub>H<sub>12</sub>BrF<sub>6</sub>N<sub>3</sub>O<sub>2</sub>

Synonyms:C₁₅H₁₂BrF₆N₃O₂

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Chemical Property of C₁₅H₁₂BrF₆N₃O₂

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Technology Process of C₁₅H₁₂BrF₆N₃O₂

There total 4 articles about C₁₅H₁₂BrF₆N₃O₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 1400916-99-5
C₁₅H₁₃F₆N₃O₃

: 1400917-00-1
C₁₅H₁₂BrF₆N₃O₂

Guidance literature:: With carbon tetrabromide; triphenylphosphine; In acetonitrile; at 65 ℃; for 14h;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1535-73-5
m-trifluoromethoxyaniline

: 1400917-00-1
C₁₅H₁₂BrF₆N₃O₂

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; benzotriazol-1-ol / N,N-dimethyl-formamide / 60 h / 80 °C

2: sodium tetrahydroborate / methanol / 24 h / 20 °C

3: triphenylphosphine; carbon tetrabromide / acetonitrile / 14 h / 65 °C

With sodium tetrahydroborate; carbon tetrabromide; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triphenylphosphine; In methanol; N,N-dimethyl-formamide; acetonitrile;
DOI:10.1016/j.tet.2012.07.069

Reference yield:

: 1400916-93-9
C₁₆H₁₃F₆N₃O₄

: 1400917-00-1
C₁₅H₁₂BrF₆N₃O₂

Guidance literature:: Multi-step reaction with 2 steps

1: sodium tetrahydroborate / methanol / 24 h / 20 °C

2: triphenylphosphine; carbon tetrabromide / acetonitrile / 14 h / 65 °C

With sodium tetrahydroborate; carbon tetrabromide; triphenylphosphine; In methanol; acetonitrile;
DOI:10.1016/j.tet.2012.07.069