8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside

Base Information

• Chemical Name: 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside
• CAS No.: 107342-86-9
• Molecular Formula: C₃₇H₅₂O₈
• Molecular Weight: 624.815
• Mol file: 107342-86-9.mol

Synonyms:8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside

Chemical Property of 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside

Chemical Property:

Purity/Quality:

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Technology Process of 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside

There total 1 articles about 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

8-ethoxycarbonyloctanol (3639-34-7) + 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranosyl bromide (89067-96-9) → 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-β-D-mannopyranoside (107342-93-8) + 8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside (107342-86-9)

Guidance literature:

With silver silicate; 4 A molecular sieve; In 1,2-dichloro-ethane; at 0 - 20 ℃; for 2.5h;

DOI:10.1016/S0008-6215(00)90297-0

Reference yield: 60.0%

8-ethoxycarbonyloctyl 3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranoside (107342-86-9) → 8-ethoxycarbonyloctyl 2,4-di-O-benzyl-α-D-mannopyranoside (108400-02-8)

Guidance literature:

With sodium acetate; palladium dichloride; In water; acetic acid; at 80 ℃; for 1h;

DOI:10.1016/S0008-6215(00)90297-0

upstream raw materials:

8-ethoxycarbonyloctanol

3,6-di-O-allyl-2,4-di-O-benzyl-α-D-mannopyranosyl bromide

Downstream raw materials:

8-ethoxycarbonyloctyl 2,4-di-O-benzyl-α-D-mannopyranoside