1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Base Information

Chemical Name:1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene
CAS No.:1315484-00-4
Molecular Formula:C₁₉H₁₉N₅
Molecular Weight:317.393
Hs Code.:

Synonyms:1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

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Chemical Property of 1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

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Technology Process of 1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

There total 3 articles about 1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 9.0%

: 1315483-79-4
1-(3R)-piperidin-3-yl-1,6-dihydro-imidazo[4,5-d]pyrrolo[2,3-b]pyridine

: 98-80-6
phenylboronic acid

: 1315484-00-4
1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: With oxygen; copper(II) acetate monohydrate; In dichloromethane; at 40 ℃; for 78h; Molecular sieve; Sealed tube;

Reference yield:

: 1315483-76-1
1-[(3R)-1-(phenylmethyl)-piperidin-3-yl]-1,6-dihydro-imidazo[4,5-d]pyrrolo[2,3-b]pyridine

: 1315484-00-4
1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: Multi-step reaction with 2 steps

1: ammonium formate / palladium hydroxide, 20 wt% on carbon / methanol / 1.5 h / Reflux

2: oxygen / copper(II) acetate monohydrate / dichloromethane / 78 h / 40 °C / Molecular sieve; Sealed tube

With oxygen; ammonium formate; palladium hydroxide, 20 wt% on carbon; copper(II) acetate monohydrate; In methanol; dichloromethane;

Reference yield:

: 1315494-63-3
1-[(3R)-1-(phenylmethyl)-piperidin-3-yl]-6-(phenylsulfonyl)-1,6-dihydro-imidazo[4,5-d]pyrrolo[2,3-b]pyridine

: 1315484-00-4
1-((R)-1-phenyl-piperidin-3-yl)-1,6-dihydro-1,3,5,6-tetraaza-as-indacene

Guidance literature:: Multi-step reaction with 3 steps

1: sodium hydroxide / methanol; water / 7 h / 20 °C

2: ammonium formate / palladium hydroxide, 20 wt% on carbon / methanol / 1.5 h / Reflux

3: oxygen / copper(II) acetate monohydrate / dichloromethane / 78 h / 40 °C / Molecular sieve; Sealed tube

With oxygen; ammonium formate; sodium hydroxide; palladium hydroxide, 20 wt% on carbon; copper(II) acetate monohydrate; In methanol; dichloromethane; water;