2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

Base Information

Chemical Name:2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride
CAS No.:1421502-03-5
Molecular Formula:C₅₅H₄₅Cl₃N₂Ni
Molecular Weight:899.025
Hs Code.:

Synonyms:2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

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Chemical Property of 2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

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Technology Process of 2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

There total 3 articles about 2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 77.0%

: 29046-78-4
(1,2-dimethoxyethane)dichloronickel(II)

: 2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenamine

: 1421502-03-5
2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

Guidance literature:: In dichloromethane; at 20 ℃; Inert atmosphere; Schlenk technique;
DOI:10.1016/j.jorganchem.2012.12.009

Reference yield:

: 1373618-99-5
2,6-bis(diphenylmethyl)-4-chloro-benzenamine

: 1421502-03-5
2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 3 h / Reflux

2: toluene-4-sulfonic acid / toluene / 120 °C

3: dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With toluene-4-sulfonic acid; In dichloromethane; toluene;
DOI:10.1016/j.jorganchem.2012.12.009

Reference yield:

: 82-86-0
acenaphthene quinone

: 1421502-03-5
2,6-dibenzhydryl-N-(2-(2,6-diethyl-4-methylphenylimino)acenaphthylenylidne)-4-chlorobenzenaminonickel dichloride

Guidance literature:: Multi-step reaction with 3 steps

1: toluene-4-sulfonic acid / toluene / 3 h / Reflux

2: toluene-4-sulfonic acid / toluene / 120 °C

3: dichloromethane / 20 °C / Inert atmosphere; Schlenk technique

With toluene-4-sulfonic acid; In dichloromethane; toluene;
DOI:10.1016/j.jorganchem.2012.12.009