C₅₉H₄₇N₃O₂Si

Base Information

• Chemical Name: C₅₉H₄₇N₃O₂Si
• CAS No.: 1402087-19-7
• Molecular Formula: C₅₉H₄₇N₃O₂Si
• Molecular Weight: 858.127
• Mol file: 1402087-19-7.mol

Synonyms:C₅₉H₄₇N₃O₂Si

Chemical Property of C₅₉H₄₇N₃O₂Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₅₉H₄₇N₃O₂Si

There total 4 articles about C₅₉H₄₇N₃O₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

1,1-dimethyl-3,4-diphenyl-2-(4-biphenyl-2,2':6',2''-terpyridine)-5-(p-bromophenyl)silole (1383581-82-5) + 3,4-Dimethoxyphenylboronic acid (122775-35-3) → C59H47N3O2Si (1402087-19-7)

Guidance literature:

With tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; for 72h; Inert atmosphere; Reflux;

DOI:10.1016/j.dyepig.2012.04.007

Reference yield:

C18H16Cl2SiZn2 (333174-61-1) → C59H47N3O2Si (1402087-19-7)

Guidance literature:

Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; 2: Suzuki coupling / 3: Suzuki coupling;

DOI:10.1016/j.dyepig.2012.04.007

Reference yield:

1.4-dibromobenzene (106-37-6) → C59H47N3O2Si (1402087-19-7)

Guidance literature:

Multi-step reaction with 3 steps

1: bis-triphenylphosphine-palladium(II) chloride

2: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

3: tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate / tetrahydrofuran; water / 72 h / Inert atmosphere; Reflux

With bis-triphenylphosphine-palladium(II) chloride; tetrakis(triphenylphosphine) palladium⁽⁰⁾; potassium carbonate; In tetrahydrofuran; water; 2: Suzuki coupling / 3: Suzuki coupling;

DOI:10.1016/j.dyepig.2012.04.007

upstream raw materials:

1,1-dimethyl-2,5-bis(4'-bromophenyl)-3,4-diphenylsilole

C₁₈H₁₆Cl₂SiZn₂

1,1-dimethyl-3,4-diphenyl-2-(4-biphenyl-2,2':6',2''-terpyridine)-5-(p-bromophenyl)silole

3,4-Dimethoxyphenylboronic acid