N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

Base Information

Chemical Name:N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester
CAS No.:138093-84-2
Molecular Formula:C₃₁H₄₉N₅O₁₀
Molecular Weight:651.758
Hs Code.:

N-(benzyloxycarbonyl)-D-alanyl-N<sup>β</sup>-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N<sup>ε</sup>-(tert-butoxycarbonyl)-D-lysine methyl ester

Synonyms:N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

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Chemical Property of N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

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Technology Process of N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

There total 4 articles about N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 138093-84-2
N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N / tetrahydrofuran; H₂O / 5 h / Ambient temperature

2: 85 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (WSC*HCl) / CH₂Cl₂ / 2.5 h / Ambient temperature

3: H₂ / 10percent Pd/C / methanol / 17 h / 760 Torr / Ambient temperature

4: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (WSC*HCl) / CH₂Cl₂ / 1.5 h / Ambient temperature

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; dichloromethane; water;
DOI:10.1021/ja00029a031

Reference yield:

: 16947-84-5,62234-36-0
N-[(benzyloxy)carbonyl]-3-[(tert-butoxycarbonyl)amino]-L-alanine

: 138093-84-2
N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 85 percent / 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (WSC*HCl) / CH₂Cl₂ / 2.5 h / Ambient temperature

2: H₂ / 10percent Pd/C / methanol / 17 h / 760 Torr / Ambient temperature

3: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (WSC*HCl) / CH₂Cl₂ / 1.5 h / Ambient temperature

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00029a031

Reference yield:

: 130581-88-3
N^α-(benzyloxycarbonyl)-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

: 138093-84-2
N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10percent Pd/C / methanol / 17 h / 760 Torr / Ambient temperature

2: 1-ethyl-3-<3-(dimethylamino)propyl>carbodiimide hydrochloride (WSC*HCl) / CH₂Cl₂ / 1.5 h / Ambient temperature

With hydrogen; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; palladium on activated charcoal; In methanol; dichloromethane;
DOI:10.1021/ja00029a031

upstream raw materials:

N-benzyloxycarbonyl-D-alanine

di-tert-butyl dicarbonate

N-[(benzyloxy)carbonyl]-3-[(tert-butoxycarbonyl)amino]-L-alanine

N^α-(benzyloxycarbonyl)-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

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Encyclopedia

Technology Process of N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

NAVIGATION

Encyclopedia

Technology Process of N-(benzyloxycarbonyl)-D-alanyl-Nβ-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-Nε-(tert-butoxycarbonyl)-D-lysine methyl ester

N-(benzyloxycarbonyl)-D-alanyl-Nβ-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-Nε-(tert-butoxycarbonyl)-D-lysine methyl ester

NAVIGATION

Technology Process of N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester

N-(benzyloxycarbonyl)-D-alanyl-N^β-(tert-butoxycarbonyl)-L-α,β-diaminopropionyl-N^ε-(tert-butoxycarbonyl)-D-lysine methyl ester