8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Base Information

Chemical Name:8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine
CAS No.:61774-75-2
Molecular Formula:C₂₆H₁₉NO₄
Molecular Weight:409.441
Hs Code.:

8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzo<c>phenanthridine

Synonyms:8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Suppliers and Price of 8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

There total 15 articles about 8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.9%

: 54354-62-0
decarine

: 100-44-7
benzyl chloride

: 61774-75-2
8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Guidance literature:: With potassium carbonate; In N,N-dimethyl-formamide; at 50 ℃; for 4h;

Reference yield: 62.0%

: 95712-58-6
N-<3'-(benzyloxy)-6'-bromo-2'-methoxybenzyl>-6,7-(methylenedioxy)-1-naphthylamine

: 61774-75-2
8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Guidance literature:: With ammonia; potassium amide; In diethyl ether;
DOI:10.1021/jo00243a020

Reference yield:

: 53811-49-7
naphtho[2,3-d][1,3]dioxol-5-amine

: 61774-75-2
8-(benzyloxy)-7-methoxy-2,3-(methylenedioxy)benzophenanthridine

Guidance literature:: Multi-step reaction with 3 steps

1: toluene / 1 h / Heating

2: dimethylaminoborane, acetic acid / toluene / 1 h

3: 25 percent / tri-n-octyltin hydride, azobis(2-methylbutyronitrile) / toluene / 0.5 h / 110 °C

With dimethylamine borane; azobis(2-cyanobutane); tri-n-octyltin hydride; acetic acid; In toluene;
DOI:10.1021/np980193s