1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

Base Information

Chemical Name:1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid
CAS No.:136494-26-3
Molecular Formula:C₂₆H₃₈N₂O₄
Molecular Weight:442.599
Hs Code.:

Synonyms:1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

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Chemical Property of 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

Chemical Property:

Purity/Quality:

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Technology Process of 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

There total 5 articles about 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 136494-24-1
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoate

: 136494-26-3
1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

Guidance literature:: With water; potassium carbonate; In methanol; for 1h; Yield given; Heating;
DOI:10.1002/ardp.2503240802

Reference yield:

: 65706-29-8
diethyl 2-(3-cyclohexyl-3-hydroxypropyl)aminononanedioate

: 136494-26-3
1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: toluene / 2 h / Ambient temperature

2: 1,8-diazabicyclo<5.4.0>undec-7-ene / toluene / 1.) room temp., 16 h 2.) 60 deg C, 1 h

3: 56 percent / NaBH₄, acetic acid / propan-2-ol / 1.) 3 h 2.) room temp., overnight

4: water, K₂CO₃ / methanol / 1 h / Heating

With sodium tetrahydroborate; water; potassium carbonate; acetic acid; 1,8-diazabicyclo[5.4.0]undec-7-ene; In methanol; isopropyl alcohol; toluene;
DOI:10.1002/ardp.2503240802

Reference yield:

: 136494-22-9,136494-23-0
ethyl 1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2,5-dioxo-4-imidazolidineheptanoate

: 136494-26-3
1-benzyl-3-(3-cyclohexyl-3-hydroxypropyl)-2-oxo-4-imidazolineheptanoic acid

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / NaBH₄, acetic acid / propan-2-ol / 1.) 3 h 2.) room temp., overnight

2: water, K₂CO₃ / methanol / 1 h / Heating

With sodium tetrahydroborate; water; potassium carbonate; acetic acid; In methanol; isopropyl alcohol;
DOI:10.1002/ardp.2503240802