3-phenoxycinnamyl alcohol

Base Information

• Chemical Name: 3-phenoxycinnamyl alcohol
• CAS No.: 83106-10-9
• Molecular Formula: C₁₅H₁₄O₂
• Molecular Weight: 226.275

Synonyms:3-phenoxycinnamyl alcohol

Chemical Property of 3-phenoxycinnamyl alcohol

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of 3-phenoxycinnamyl alcohol

There total 2 articles about 3-phenoxycinnamyl alcohol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

3-Phenoxybenzaldehyde (39515-51-0) → 3-phenoxycinnamyl alcohol (83106-10-9)

Guidance literature:

Multi-step reaction with 2 steps

1: neat (no solvent)

2: diisobutylaluminium hydride / dichloromethane

With diisobutylaluminium hydride; In dichloromethane;

DOI:10.1021/acs.orglett.6b03836

Reference yield:

(E)-3-(3-Phenoxy-phenyl)-acrylic acid ethyl ester → 3-phenoxycinnamyl alcohol (83106-10-9)

Guidance literature:

With diisobutylaluminium hydride; In dichloromethane;

DOI:10.1021/acs.orglett.6b03836 DOI:10.1002/adsc.201801389

Reference yield: 72.0%

3-phenoxycinnamyl alcohol (83106-10-9) + Methyl phenyldiazoacetate (22979-35-7) → methyl 2-hydroxy-3-(3-phenoxyphenyl)-2-phenylpent-4-enoate

Guidance literature:

With (tricyclohexylphosphine)gold(I) chloride; silver(I) triflimide; In diethyl ether; at 20 ℃; for 3h; diastereoselective reaction;

DOI:10.1021/acs.orglett.6b03836

upstream raw materials:

3-Phenoxybenzaldehyde

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