(1R)-1-(3-hydroxyphenyl)-2-ethanol

Base Information

• Chemical Name: (1R)-1-(3-hydroxyphenyl)-2-ethanol
• CAS No.: 112023-62-8
• Molecular Formula: C₁₄H₂₂N₂O₃
• Molecular Weight: 266.34

Synonyms:(1R)-1-(3-hydroxyphenyl)-2-ethanol

Chemical Property of (1R)-1-(3-hydroxyphenyl)-2-ethanol

Chemical Property:

Purity/Quality:

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Technology Process of (1R)-1-(3-hydroxyphenyl)-2-ethanol

There total 2 articles about (1R)-1-(3-hydroxyphenyl)-2-ethanol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 76.0%

phenylephrine hydrochloride (61-76-7,827-62-3) + N,N-diethylcarbamyl chloride (88-10-8) → (1R)-1-(3-hydroxyphenyl)-2-ethanol (112023-62-8)

Guidance literature:

With triethylamine; In tetrahydrofuran; for 1h;

DOI:10.1021/jm00394a026

Reference yield: 76.0%

→ (1R)-1-(3-hydroxyphenyl)-2-ethanol (112023-62-8)

Guidance literature:

Reference yield: 64.0%

2-chloromethyl-1-methyl-1H-benzimidazole (4760-35-4) + (1R)-1-(3-hydroxyphenyl)-2-ethanol (112023-62-8) → 1,1-Diethyl-3-{(R)-2-hydroxy-2-[3-(1-methyl-1H-benzoimidazol-2-ylmethoxy)-phenyl]-ethyl}-3-methyl-urea (110193-15-2)

Guidance literature:

With caesium carbonate; In acetone; for 48h; Heating;

DOI:10.1021/jm00394a026

upstream raw materials:

phenylephrine hydrochloride

N,N-diethylcarbamyl chloride

Downstream raw materials:

N-{(R)-2-Hydroxy-2-[3-(1-methyl-1H-benzoimidazol-2-ylmethoxy)-phenyl]-ethyl}-N-methyl-propionamide

(1R)-1-<3-(2-quinolinylmethoxy)phenyl>-2-ethanol

(1R)-1-[3-[(2-Benzthiazolyl)-methoxy]phenyl]-2-(N-methyl-N-diethylcarbamoyl)amino ethanol

1,1-Diethyl-3-{(R)-2-hydroxy-2-[3-(1-methyl-1H-benzoimidazol-2-ylmethoxy)-phenyl]-ethyl}-3-methyl-urea

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