4-nitrophenyl 4'-phenyl sulfone

Base Information

Chemical Name:4-nitrophenyl 4'-phenyl sulfone
CAS No.:133041-84-6
Molecular Formula:C₁₆H₁₆Cl₂N₂O₄S
Molecular Weight:403.286
Hs Code.:

4-nitrophenyl 4'-<bis(2-chloroethyl)amino>phenyl sulfone

Synonyms:4-nitrophenyl 4'-phenyl sulfone

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Chemical Property of 4-nitrophenyl 4'-phenyl sulfone

Chemical Property:

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Technology Process of 4-nitrophenyl 4'-phenyl sulfone

There total 5 articles about 4-nitrophenyl 4'-phenyl sulfone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 133041-83-5
4-nitrophenyl 4'-phenyl sulfide

: 133041-84-6
4-nitrophenyl 4'-phenyl sulfone

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; at 20 ℃; for 1h;
DOI:10.1021/jm00109a005

Reference yield: 96.0%

: 189638-99-1
N,N-bis-(2-chloroethyl)-4-(4-nitrophenylsulfinyl)aniline

: 133041-84-6
4-nitrophenyl 4'-phenyl sulfone

Guidance literature:: With ammonium molybdate; dihydrogen peroxide; In acetone; at 20 ℃; for 5h;
DOI:10.1021/jm9904957

Reference yield:

: 101-59-7
4-amino-4'-nitrodiphenyl sulfide

: 133041-84-6
4-nitrophenyl 4'-phenyl sulfone

Guidance literature:: Multi-step reaction with 4 steps

1: 80.4 percent / AcOH / tetrahydrofuran / 168 h / 20 °C

2: 80.2 percent / POCl₃ / 0.67 h / Heating

3: 97.1 percent / 30percent aq. H₂O₂; TFA / 2.5 h / 0 °C

4: 96 percent / aq. H₂O₂; ammonium molybdate / acetone / 5 h / 20 °C

With ammonium molybdate; dihydrogen peroxide; acetic acid; trifluoroacetic acid; trichlorophosphate; In tetrahydrofuran; acetone;
DOI:10.1021/jm9904957