2-Bromo-3-cyclohexylprop-2-en-1-ol

Base Information

Chemical Name:2-Bromo-3-cyclohexylprop-2-en-1-ol
CAS No.:127652-85-1
Molecular Formula:C₉H₁₅BrO
Molecular Weight:219.121
Hs Code.:
DSSTox Substance ID:DTXSID70698478
Mol file:127652-85-1.mol

Synonyms:127652-85-1;DTXSID70698478;2-Bromo-3-cyclohexylprop-2-en-1-ol;FT-0770494

Suppliers and Price of 2-Bromo-3-cyclohexylprop-2-en-1-ol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-BROMO-3-CYCLOHEXYL-PROP-2-EN-1-OL 95.00%
5MG
$ 501.01

Total 1 raw suppliers

Chemical Property of 2-Bromo-3-cyclohexylprop-2-en-1-ol

Chemical Property:

Vapor Pressure:0.00067mmHg at 25°C
Boiling Point:274.8°Cat760mmHg
Flash Point:120°C
PSA：20.23000
Density:1.433g/cm³
LogP:2.83780
XLogP3:3.1
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:218.03063
Heavy Atom Count:11
Complexity:137

Purity/Quality:: 2-BROMO-3-CYCLOHEXYL-PROP-2-EN-1-OL 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1CCC(CC1)C=C(CO)Br

Technology Process of 2-Bromo-3-cyclohexylprop-2-en-1-ol

There total 1 articles about 2-Bromo-3-cyclohexylprop-2-en-1-ol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2043-61-0
cyclohexanecarbaldehyde

: 127652-85-1
(E)-2-bromo-3-cyclohexylallyl alcohol

Guidance literature:: DOI:10.1016/S0040-4039(01)80544-X

Reference yield:

: 127652-85-1
(E)-2-bromo-3-cyclohexylallyl alcohol

: 127652-89-5,127652-90-8
(1E,7Z)-(3R,4R)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-1-cyclohexyl-4-methyl-deca-1,7-dien-3-ol

Guidance literature:: Multi-step reaction with 3 steps

1: tret-butyllithium / diethyl ether / -78 - 24 °C

3: 29 percent / Et₃N / DMAP / CH₂Cl₂ / 24 °C

With tert.-butyl lithium; triethylamine; dmap; In diethyl ether; dichloromethane;
DOI:10.1016/S0040-4039(01)80544-X

Reference yield:

: 127652-85-1
(E)-2-bromo-3-cyclohexylallyl alcohol

: 127652-89-5,127652-90-8
(1E,7Z)-(3R,4S)-2-(tert-Butyl-dimethyl-silanyloxymethyl)-1-cyclohexyl-4-methyl-deca-1,7-dien-3-ol

Guidance literature:: Multi-step reaction with 5 steps

1: tret-butyllithium / diethyl ether / -78 - 24 °C

3: 29 percent / Et₃N / DMAP / CH₂Cl₂ / 24 °C

4: 8 percent / Pd(OAc)2 / dimethylsulfoxide / 24 h / 24 °C

5: 33 percent / L-seletride / -78 °C

With tert.-butyl lithium; L-Selectride; triethylamine; dmap; palladium diacetate; In diethyl ether; dichloromethane; dimethyl sulfoxide;
DOI:10.1016/S0040-4039(01)80544-X