4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

Base Information

Chemical Name:4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide
CAS No.:102670-54-2
Molecular Formula:C₁₆H₂₄ClN₃O₄
Molecular Weight:357.837
Hs Code.:

Synonyms:4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

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Chemical Property of 4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

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Technology Process of 4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

There total 3 articles about 4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 38339-95-6
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-hydroxybenzamide

: 96-32-2
bromoacetic acid methyl ester

: 102670-54-2
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

Guidance literature:: With sodium hydride; In N,N-dimethyl-formamide; for 16h; Ambient temperature;
DOI:10.1021/jm00403a011

Reference yield:

: 96-32-2
bromoacetic acid methyl ester

: 38059-78-8
4-amino-5-chloro-N-<2-(diethylamino)ethyl>-2-hydroxybenzamide hydrochloride

: 102670-54-2
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

Guidance literature:: In water; N,N-dimethyl-formamide;

Reference yield:

: 364-62-5
metoclopramide

: 102670-54-2
4-amino-5-chloro-N-[2-(diethylamino)ethyl]-2-(2-methoxy-2-oxoethoxy)benzamide

Guidance literature:: Multi-step reaction with 2 steps

1: 98 percent / sodium hydride, ethanethiol / dimethylformamide / 1.5 h / 100 - 105 °C

2: 67 percent / sodium hydride / dimethylformamide / 16 h / Ambient temperature

With sodium hydride; ethanethiol; In N,N-dimethyl-formamide;
DOI:10.1021/jm00403a011