N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Base Information

Chemical Name:N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester
CAS No.:126216-35-1
Molecular Formula:C₂₁H₃₁N₃O₈
Molecular Weight:453.492
Hs Code.:

N-<2-<Bis(carboxymethyl)amino>ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Synonyms:N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

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Chemical Property of N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Chemical Property:

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Technology Process of N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

There total 4 articles about N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 126216-33-9
N-<2-ethyl>-N-(carboxymethyl)-4-nitro-DL-phenylalanine Tetramethyl Ester

: 126216-35-1
N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Guidance literature:: With hydrogen; palladium on activated charcoal; In methanol; under 3102.9 Torr;
DOI:10.1021/jo00296a057

Reference yield:

: 19376-45-5
tetramethyl ethylenediamine-N,N,N',N'-tetraacetate

: 126216-35-1
N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Guidance literature:: Multi-step reaction with 3 steps

1: 1) LDA / 1) THF, -78 deg C, 2) HMPA, -78 deg C -> 25 deg C

2: 1) 97percent H₂SO₄, conc. HNO₃, 2) SOCl₂ / 1) 0 deg C, 2) 0 deg C

3: H₂ / 30percent Pd/C / methanol / 3102.9 Torr

With thionyl chloride; sulfuric acid; hydrogen; nitric acid; lithium diisopropyl amide; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00296a057

Reference yield:

: 60-00-4,94108-75-5
ethylenediaminetetraacetic acid

: 126216-35-1
N-<2-ethyl>-N-(carboxymethyl)-4-amino-DL-phenylalanine Tetramethyl Ester

Guidance literature:: Multi-step reaction with 4 steps

1: 78 percent / SOCl₂

2: 1) LDA / 1) THF, -78 deg C, 2) HMPA, -78 deg C -> 25 deg C

3: 1) 97percent H₂SO₄, conc. HNO₃, 2) SOCl₂ / 1) 0 deg C, 2) 0 deg C

4: H₂ / 30percent Pd/C / methanol / 3102.9 Torr

With thionyl chloride; sulfuric acid; hydrogen; nitric acid; lithium diisopropyl amide; palladium on activated charcoal; In methanol;
DOI:10.1021/jo00296a057