tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine

Base Information

• Chemical Name: tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine
• CAS No.: 1380248-39-4
• Molecular Formula: C₃₇H₅₅O₂P
• Molecular Weight: 562.816

Synonyms:tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine

Chemical Property of tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine

Chemical Property:

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Technology Process of tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine

There total 1 articles about tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2-iodo-2’,4’,6’-triisopropyl-3,6-dimethoxybiphenyl (1070663-76-1) + tert-butyl-1-adamantylchlorophosphine (1380248-38-3) → tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine (1380248-39-4)

Guidance literature:

2-iodo-2’,4’,6’-triisopropyl-3,6-dimethoxybiphenyl; With tert.-butyl lithium; In toluene; pentane; at -78 ℃; for 0.666667h; Inert atmosphere;

tert-butyl-1-adamantylchlorophosphine; With copper(l) chloride; In toluene; pentane; at -78 - 140 ℃; for 24h; Inert atmosphere;

DOI:10.1002/anie.201201244

Reference yield: 60.0%

tert-butyl-adamantyl(2',4',6'-triisopropyl-3,6-dimethoxybiphenyl-2-yl)phosphine (1380248-39-4) + di(2-(2′-amino-1,1′-biphenyl))palladium(II) methanesulfonate dimer → C12H10N(1-)*CH3O3S(1-)*Pd(2+)*C37H55O2P

Guidance literature:

In dichloromethane; at 20 ℃; Schlenk technique; Inert atmosphere; Sealed tube;

DOI:10.1021/acs.orglett.8b00325

upstream raw materials:

2-iodo-2’,4’,6’-triisopropyl-3,6-dimethoxybiphenyl

tert-butyl-1-adamantylchlorophosphine

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