(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

Base Information

Chemical Name:(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid
CAS No.:787623-89-6
Molecular Formula:C₃₄H₃₂N₂O₆
Molecular Weight:564.638
Hs Code.:

Synonyms:(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

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Chemical Property of (4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

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Technology Process of (4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

There total 2 articles about (4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 46755-94-6
(S)-1,1-diphenyl-1,2-propanediol

: 26339-42-4,26340-00-1
(4S,5R)-1,3-dibenzyl-1H-furo[3,4-d]imidazole-2,4,6-trione

: 787623-89-6
(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

Guidance literature:: With tributyl-amine; In toluene; at -10 ℃; for 18h; Molecular sieve; Inert atmosphere; Large scale;
DOI:10.1080/00304948.2015.1025640

Reference yield:

: 51591-75-4,634188-82-2
cis-1,3-dibenzyl-2-oxoimidazolidine-4,5-dicarboxylic acid

: 787623-89-6
(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

Guidance literature:: Multi-step reaction with 2 steps

1: toluene / 10 h / Reflux

2: tributyl-amine / toluene / 18 h / -10 °C / Molecular sieve; Inert atmosphere; Large scale

With tributyl-amine; In toluene;
DOI:10.1080/00304948.2015.1025640

Reference yield: 95.0%

: 787623-89-6
(4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid

: 28092-62-8
(3aS,6aR)-1,3-dibenzyltetrahydro-1H-furo[3,4-d]imidazole-2,4-dione

: 46755-94-6
(S)-1,1-diphenyl-1,2-propanediol

Guidance literature:: (4S,5R)-1,3-dibenzyl-5-[(S)-(1-hydroxy-1,1-diphenylpropan-2-yloxy)carbonyl]-2-oxoimidazolidine-4-carboxylic acid; With lithium hydroxide monohydrate; In tetrahydrofuran; at 25 ℃; for 3h; Large scale;

With lithium borohydride; In tetrahydrofuran; for 2h; stereoselective reaction; Reflux; Large scale;
DOI:10.1080/00304948.2015.1025640